** NCH users should use "Off-Campus Consortium (Non-OSU Ohio Universities)" as they are eligible for internal/consortium rate structure
Please Note - Electronic Service Forms
Please only submit service requests when you are ready to submit/send samples.
For External Users:
Directions to submit a Service Request Form and samples to MS&P Faclity
OSU Sponsored Guest Account / FOM Profile and Account Form
Go to FOM to: add/inactivate existing account information, change profile information, view your Forms submitted to MS&P Facility, view billing information.
When submitting multiple samples, please fill out only one (1) Service Request Form in FOM and attach all sample information in a separate document. Please do not submit multiple forms. If you run into problems with FOM please contact firstname.lastname@example.org.
FY2020 BILLING RATES (Effective August 21st, 2019)
* includes NCH
|Academic/Non-profit (Outside OH Consortium) Rates||Industry|
|Molecular weight/Chemical Formula determination|
|Accurate mass (FT-ICR and XL)||Sample||$50.00||$90.00||$170.00|
|Nominal mass (Amazon, UltrafleXtreme (TOF-TOF)||Sample||$40.00||$70.00||$110.00|
|LC-MS injection (< 10 samples, each injection), quantitative||Injection||$120.00||$180.00||$280.00|
|LC-MS injection (>10 samples, each injection), quantitative||Injection||$100.00||$150.00||$250.00|
|LC-MS injection (< 10 samples, each injection), qualitative||Injection||$140.00||$280.00||$350.00|
|LC-MS injection (>10 samples, each injection), qualitative||Injection||$120.00||$200.00||$300.00|
|Large molecules (>10,000 Da) MALDI TOF-TOF||Sample||$150.00||$500.00||$800.00|
|Small molecules (<10,000 Da), high resolution FT-ICR||Sample||$300.00||$550.00||$900.00|
|Self operation and Staff time (per hour)|
|Self operation Amazon (min 1/2 hr increments)||Hour||$5.00||$15.00||$50.00|
|Self operation MALDI TOF-TOF, Quantiva (min 1/2 hr increments)||Hour||$15.00||$30.00||$80.00|
|Self operation Orbis, Fusion, ICR (min 1/2 hr increments)||Hour||$20.00||$50.00||$120.00|
|1D SDS-PAGE - 10 Wells||Sample||$60.00||$100.00||$200.00|
|Peptide/Protein Enrichment, e.g., Phosphorylation||Sample||$50.00||$80.00||$120.00|
|Coommassie Stain (Includes Image Acquisition)||Gel||$60.00||$120.00||$300.00|
|Protein Quantitation (Bradford), Peptide desalting||Sample||$20.00||$40.00||$100.00|
|LC-MS/MS Peptide Sequencing - Long Gradient (> 2hrs) - Fusion/QE||Sample||$250.00||$350.00||$800.00|
|LC-MS/MS Peptide Sequencing - Reg Gradient (2hrs) - Fusion/QE||Sample||$200.00||$280.00||$350.00|
|LC-MS/MS Peptide Sequencing - Reg Gradient (1hrs) - Fusion/QE||Sample||$150.00||$220.00||$280.00|
|LC-MS/MS - 2D or off line LC Fractions (per fraction) - Fusion/QE||Fraction||$100.00||$180.00||$300.00|
|Top Down Proteomics (Fusion, QE or ICR)||Sample||$500.00||$800.00||$1500.00|
|tims TOF Pro bottom up||Sample||$300.00||$400.00||$600.00|
Sample Submission Guidelines
Samples can be brought to 250 Biomedical Research Tower, along with a filled out sample submission form, weekdays between 8 am and 5 pm. We have a refrigerator, freezer and dry box for samples that require special storage. It is preferred if samples are submitted neat or dried down, typically ug amounts is all that is needed.
Biological samples are handled differently and require different conditions. Salts, buffers and surfactants suppress ionization and need to be removed for mass spec analysis. When possible, it is advised to dialyze the sample into nanopure or at least distilled water prior to submission. We also have several de-salting techniques for proteins and oligonucleotides available in our facility. List all salts, buffers and detergents the protein or oligonucleotide is in, or has recently been in. For optimal results, please discuss your project with Dr. Somogyi prior to submission. Certain classes of proteins need to be handled differently than others, the more we know about your system, the better the data. Protein samples for ESI are prepared in 50% acetonitrile 50% water with 0.1% formic acid. Slightly acidic conditions are necessary to facilitate protonation
We CANNOT run samples that are in aromatic solvents like benzene, toluene, or solvents such as DMSO and DMF.
Electrospray and MALDI samples are prepared in Methanol, Acetonitrile, water, THF, chloroform. We will acidify the sample with acetic or formic acid unless you indicate the sample is acid sensitive.
Turn around times vary between 1 day to a week depending on sample load, instrument availability and type of analysis. We will email you when the results are ready to be picked up.